HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 45080638, compound → HCID 54704662, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 45080638 | HCID 45080638 | — |
| Reactant | HCID 54691713 | HCID 54691713 | — |
| Product | HCID 54704662 | HCID 54704662 | — |
Reaction Steps
Compound 757 was prepared from 4-{4-[(3,4-dichloro-benzyl)-methyl-carbamoyl]-3-hydroxy-2-oxo-2,5-dihydro-pyrrol-1-yl}-butyric acid and 1-phenyl-cyclopropanesulfonic acid amide using the method described for compound 751. The title compound was purified by preparative HPLC (C18, ODS-A, S-75 μm, 50% acetonitrile/water/0.5% TFA) and isolated as a white powder (0.0026 g, 3% yield). HRMS (M−H) calcd for C26H30N3Cl2O6S: 582.12324. found: 582.1215.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07109186B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-1d78d07dac6e44c9bccbc1d9470cff1e |
| Source note | uspto-grants-2006_09 |