HuagongsheHuagongshe Chemistry Print Report · For research reference only
Gamma-Aminobutyric Acid → HCID 54691761, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Gamma-Aminobutyric Acid | HCID 119 | — |
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | HCID 69655692 | HCID 69655692 | — |
| Product | HCID 54691761 | HCID 54691761 | 55% |
Reaction Steps
2-Hydroxy-3-(methyl-naphthalen-1-ylmethyl-carbamoyl)-acrylic acid methyl ester was treated with paraformaldehyde and 4-amino-butyric acid according to the procedure described in the preparation of compound 12 to give the title compound as a white powder (0.0210 g, 55% yield). 1HNMR (300 MHz, CDCl3) δ: 7.93–7.81 (2H, m), 7.55–7.42 (4H, m), 7.42–7.28 (1H, m), 5.13 (2H, s), 4.14 (2H, s), 3.52–3.50 (2H, m), 2.36–2.29 (2H, m), 1.90–1.87 (2H, m).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07109186B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-8efb0ca05e6445f7ad47651e62321b71 |
| Source note | uspto-grants-2006_09 |