HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isobutyl chloroformate → [1,2,3]Thiadiazolo[5,4-b]pyridin-6-ylmethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isobutyl chloroformate | HCID 62365 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | [1,2,3]Thiadiazolo[5,4-b]pyridine-6-carboxylic acid | HCID 21873749 | — |
| Product | [1,2,3]Thiadiazolo[5,4-b]pyridin-6-ylmethanol | HCID 21873601 | 15.9% |
Reaction Steps
The carboxylic acid (iii) (0.82 g) was reacted with isobutylchloroformate and sodium borohydride to afford a semi-solid (0.12 g), after chromatography on silica gel (chloroform).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07109213B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-62bb8549b0bb404db31e93d18de99b8c |
| Source note | uspto-grants-2006_09 |