[1,2,3]Thiadiazolo[5,4-b]pyridin-6-ylmethanol → HCID 11355675, compound

HRID 2214965Notes

Reaction equation

HRID 2214965 reaction equation
[N:1]1[C:9]2[C:4](=[N:5][CH:6]=[C:7]([CH2:10][OH:11])[CH:8]=2)[S:3][N:2]=1>[O-2].[O-2].[Mn+4]>[N:1]1[C:9]2[C:4](=[N:5][CH:6]=[C:7]([CH:10]=[O:11])[CH:8]=2)[S:3][N:2]=1

Participants

3

Reactant 1

HCID 21873601[1,2,3]Thiadiazolo[5,4-b]pyridin-6-ylmethanol

Product 1

HCID 11355675HCID 11355675, compoundYield 51.6%

Reagents, catalysts & solvents 1

HCID 178418406HCID 178418406, compoundCatalyst

Procedure

The alcohol (iv) (0.10 g) was oxidised with manganese dioxide to afford a solid (51 mg).

Sources & evidence

ORD record
ord-63eb7a7bf0c34c8d80ab82756f7c5027
Source dataset
uspto-grants-2006_09
Patent number
US07109213B2

Reaction notes

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