HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propionyl chloride → HCID 21949640, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propionyl chloride | HCID 62324 | — |
| Reactant | HCID 21949615 | HCID 21949615 | — |
| Catalyst | HCID 131725947 | HCID 131725947 | — |
| Product | HCID 21949640 | HCID 21949640 | — |
Reaction Steps
was prepared in analogy to example 59, but starting the reaction sequence with propionyl chloride instead of isobutyryl chloride, and elaborating the terminal double bond via hydroboration with 9-BBN (as described in example 53) into a primary hydroxy group instead of oxidative cleavage with OsO4/NaBH4, as off-white solid of mp. 113–17°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07109225B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-8983b5a2746c441f9f6b0643d8b17033 |
| Source note | uspto-grants-2006_09 |