HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 178427515, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | Fmoc-Pro-Pro-Arg(Pmc)-OtBu | HCID 178427514 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178427515 | HCID 178427515 | — |
Reaction Steps
Fmoc-Pro-Pro-Arg(Pmc)-OtBu 1.7 g (1.86 mmol) was dissolved in acetonitrile (50 mL) and treated with piperidine (2 mL) and the mixture was stirred at RT for 4 h. The solvents were removed and the residue was purified by chromatography using methylene chloride-methanol (8:2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07109167B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-ec91dfa785344e7db7d92f9b924c1896 |
| Source note | uspto-grants-2006_09 |