Methyldichlorosilane → HCID 21953390, compound

Participants

Reaction Steps

As in Example 1, phenylthiomethyl chloride (3.31 g, 0.0209 mol), methyldichlorosilane (7.23 g, 0.0628 mol) and tetrabutylphosphonium chloride (0.615 g, 0.00209 mol) were put in a 50 mL stainless steel tube under nitrogen atmosphere. The reaction chamber was closed with a cover and the reaction was carried out at 120° C. for 12 hours. This reaction mixture was distilled under low pressure to give 1.82 g of methyl(phenylthiomethyl)dichlorosilane in 36.9% yield.

Provenance & Evidence