HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 58700277, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-(Bromomethyl)pyridine | HCID 642799 | — |
| Reactant | HCID 58700375 | HCID 58700375 | — |
| Product | HCID 58700277 | HCID 58700277 | — |
Reaction Steps
The title compound was prepared by following the general Method C as a light yellow solid (56 mg, 57%) from (4aS,9bR)-8-hydroxy-5-methyl-6-trifluoromethyl-1,3,4,4a,5,9b-hexahydro-pyrido[4,3-b]indole-2-carboxylic acid tert-butyl ester (Example 71, 100 mg, 0.27 mmol), 4-bromomethyl-pyridine (141 mg, 0.56 mmol) and K2CO3 (156 mg, 1.12 mmol). MS (ESI): 364 (base, M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07109339B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-f4c3673e8d1f4f5fba5cd1faa14935fe |
| Source note | uspto-grants-2006_09 |