HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzo(b)thiophene-2-carboxylic acid → HCID 21942362, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzo(b)thiophene-2-carboxylic acid | HCID 95864 | — |
| Reactant | 5-Amino-2-(4-piperidinopiperidin-1-yl)benzonitrile | HCID 21942342 | — |
| Product | HCID 21942362 | HCID 21942362 | 27.4% |
Reaction Steps
By the reaction and treatment in the same manner as in Example 6 using benzo[b]thiophene-2-carboxylic acid (1.0 g) and 5-amino-2-(4-piperidinopiperidin-1-yl)benzonitrile (1.4 g), the title compound (0.6 g) was obtained. melting point: 275° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07112594B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-68770aac000f47ef8c4c200ddfa67d49 |
| Source note | uspto-grants-2006_09 |