HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 86590086, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Benzofuran-2-carboxylic acid | HCID 10331 | — |
| Reactant | 5-Amino-2-(2,2-dimethyl-3-hydroxypropoxy)benzonitrile monohydrochloride | HCID 21942317 | — |
| Product | HCID 86590086 | HCID 86590086 | — |
Reaction Steps
By the reaction and treatment in the same manner as in Example 6 using benzo[b]furan-2-carboxylic acid (0.7 g), 5-amino-2-(2,2-dimethyl-3-hydroxypropoxy)benzonitrile monohydrochloride (1.0 g) and triethylamine (0.6 ml), the title compound (0.26 g) was obtained. melting point: 199-201° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07112594B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-303cbd8d013844e89f7a6cfa3f83c3b9 |
| Source note | uspto-grants-2006_09 |