HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methoxyindan-1-one → 2-(6-methoxy-1H-inden-3-yl)propanoic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methoxyindan-1-one | HCID 78787 | — |
| Reactant | Methyl 2-bromopropionate | HCID 95576 | — |
| Product | 2-(6-methoxy-1H-inden-3-yl)propanoic Acid | HCID 21942769 | 68% |
Reaction Steps
This substrate was prepared using the same procedures as described for Examples 1 and 2a, starting with 5-methoxyl-1-indanone and methyl 2-bromopropionate. Yield: 68%. 1H NMR (CD2Cl2) δ 7.34 (d, J=9, 1H), 7.07 (d, J=2, 1H), 6.85 (dd, J=9, J=2, 1H), 6.32 (m, 1H), 3.82 (m, 4H), 3.36 (m, 2H), 1.56 (d, J=7, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07112597B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-6ea6d7be246a4ebca88aa6e338572bd4 |
| Source note | uspto-grants-2006_09 |