HCID 11409271, compound → HCID 135442683, compound

HRID 2216527Notes

Reaction equation

HRID 2216527 reaction equation
C1(N2C(C3C=CC(O)=CC=3)=CC(/C=C/C(OC)=O)=N2)CCCCC1.C([O:32][C:33]1[CH:38]=[CH:37][C:36]([C:39]2[N:43]([CH:44]3[CH2:49][CH2:48][CH2:47][CH2:46][CH2:45]3)[N:42]=[C:41](/[CH:50]=[CH:51]/[C:52]([O:54][CH3:55])=[O:53])[C:40]=2[C:56]2[CH:61]=[CH:60][CH:59]=[CH:58][CH:57]=2)=[CH:35][CH:34]=1)C1C=CC=CC=1>>[CH:44]1([N:43]2[C:39]([C:36]3[CH:37]=[CH:38][C:33]([OH:32])=[CH:34][CH:35]=3)=[C:40]([C:56]3[CH:61]=[CH:60][CH:59]=[CH:58][CH:57]=3)[C:41](/[CH:50]=[CH:51]/[C:52]([O:54][CH3:55])=[O:53])=[N:42]2)[CH2:45][CH2:46][CH2:47][CH2:48][CH2:49]1

Participants

3

Reactant 2

HCID 11409271HCID 11409271, compoundHCID 135814979HCID 135814979, compound

Product 1

HCID 135442683HCID 135442683, compoundYield 101.5%

Procedure

Phenol 8.8 was prepared from 8.6 according to the procedure described above for the preparation phenol 3.1. Thus, 8.6 (60 mg, 0.12 mmol) was debenzylated to yield 49 mg (100%) of 8.8. MS (ESI) 403.3 (MH+), 401.3 (MH−).

Workup

  1. customPhenol 8.8 was prepared from 8.6 according to the procedure

Sources & evidence

ORD record
ord-4bedc96b97234725804549e31af059ca
Source dataset
uspto-grants-2006_09
Patent number
US07112601B2

Reaction notes

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