HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 13100254, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Octahydrocoumarin | HCID 20487 | — |
| Product | HCID 13100254 | HCID 13100254 | 47.1% |
Reaction Steps
Using the same procedure as described under A) but starting with a solution consisting of octahydrocoumarine (22 g, 145 mmoles) into 58 g of acetic acid and a supported catalyst obtained according to procedure a), there were obtained (after bulb to bulb distillation at 42 mbar, oven=175°) 10.4 g of 4-(1-cyclohexen-1-yl)-2-butanone (purity: 71%; yield: 33%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07112699B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-cd7e8b36fec045e2ad4b67df48ead5ed |
| Source note | uspto-grants-2006_09 |