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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2217015Generated: October 30, 2026

Acetic Acid → HCID 13100254, compound

https://huagongshe.com/reaction/2217015

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic AcidHCID 176—
ReactantOctahydrocoumarinHCID 20487—
ProductHCID 13100254HCID 1310025447.1%

Reaction Steps

Using the same procedure as described under A) but starting with a solution consisting of octahydrocoumarine (22 g, 145 mmoles) into 58 g of acetic acid and a supported catalyst obtained according to procedure a), there were obtained (after bulb to bulb distillation at 42 mbar, oven=175°) 10.4 g of 4-(1-cyclohexen-1-yl)-2-butanone (purity: 71%; yield: 33%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07112699B2
Source datasetuspto-grants-2006_09
ORD IDord-cd7e8b36fec045e2ad4b67df48ead5ed
Source noteuspto-grants-2006_09