HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,6-Dibromohexane → 1-[4-[(6-Bromohexyl)oxy]butyl]benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,6-Dibromohexane | HCID 12368 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Benzenebutanol | HCID 76889 | — |
| Catalyst | Tetrabutylammonium hydrogen sulfate | HCID 94433 | — |
| Product | 1-[4-[(6-Bromohexyl)oxy]butyl]benzene | HCID 11012439 | — |
Reaction Steps
To a mixture of 5 ml (0.0323 mol) of 4-phenylbutanol and 10.1 ml (0.0657 mol) of 1,6-dibromohexane are added, with stirring, 8 g of powdered (0.121 mol of KOH) caustic potash, whereupon the temperature rises to about 30° C. Then 1.1 g (0.0033 mol) of tetra-n-butylammonium hydrogen sulphate are added, whereupon the temperature rises to about 65° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07112701B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-e9ea77ef3efd4d3e84488b647cbba208 |
| Source note | uspto-grants-2006_09 |