HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 11696392, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Benzotriazol-1-yloxy-tris(dimethylamino)phosphonium hexafluorophosphate | HCID 151348 | — |
| Reactant | 4-(Aminomethyl)benzene-1,2-diol--hydrogen bromide (1/1) | HCID 13343562 | — |
| Reactant | HCID 18451611 | HCID 18451611 | — |
| Product | HCID 11696392 | HCID 11696392 | — |
Reaction Steps
The compound was prepared based on the methodology in Example 5 using 38 mg (0.15 mmol) of 5-(4-hydroxy-3,5-dimethoxyphenyl)-penta-2E,4E-dienoic acid [Example 4], 67 mg (0.30 mmol) of 3,4 dihydroxybenzylamine hydrobromide, 153 μl (1.5 mmol) of triethylamine, and 100 mg (0.23 mmol) of BOP reagent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07407989B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-72f0b3bde23f489e8bb7f9d6ca6ddde4 |
| Source note | uspto-grants-2008_08 |