HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 11223003, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 11651470 | HCID 11651470 | — |
| Reactant | HCID 68810268 | HCID 68810268 | — |
| Product | HCID 11223003 | HCID 11223003 | 29.7% |
Reaction Steps
Prepared according to the method of example 7 (b), using N-[6-chloro-5-[(cyclohexylacetyl)amino]-2-quinolinyl]-β-alanine, 1,1-dimethylethyl ester (Example 41 (a)) (150 mg) and trifluoroacetic acid (2 mL). Purification by HPLC (Symmetry—0.1% aqueous ammonium acetate/acetonitrile) afforded the title product (39 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07408065B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-2bf95998f40149abaf2a8a4cbfd0617d |
| Source note | uspto-grants-2008_08 |