HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Proline 1,1-dimethylethyl ester → HCID 68808739, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Proline 1,1-dimethylethyl ester | HCID 6453108 | — |
| Reactant | 2,6-dichloro-N-(cyclohexylmethyl)-5-quinolinecarboxamide | HCID 86013022 | — |
| Product | HCID 68808739 | HCID 68808739 | — |
Reaction Steps
Prepared according to the method of example 30, using 2,6-dichloro-N-(cyclohexylmethyl)-5-quinolinecarboxamide Example 43(a)) (200 mg) and L-proline, 1,1-dimethylethyl ester (305 mg). Purification (SiO2, ethyl acetate:isohexane 20:80 as eluant) gave the sub-title compound as an oil (200 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07408065B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-41d6a7cb491d46e5b4b1a504847c93b2 |
| Source note | uspto-grants-2008_08 |