HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Thiophenemethylamine → 3-Nitro-4-[(3-thienylmethyl)amino]-N,N-bis(2,2,2-trifluoroethyl)benzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Thiophenemethylamine | HCID 2776381 | — |
| Edukt | 4-Fluoro-3-nitro-N,N-bis(2,2,2-trifluoroethyl)benzamide | HCID 58911744 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 3-Nitro-4-[(3-thienylmethyl)amino]-N,N-bis(2,2,2-trifluoroethyl)benzamide | HCID 58874497 | — |
Reaktionsschritte
Following the general procedure for Intermediate 2 using 4-fluoro-3-nitro-N,N-bis(2,2,2-trifluoroethyl)benzamide (125 mg, 0.359 mmol) and 3-thienylmethylamine (49 mg, 0.431 mmol) in 3 mL of EtOH containing TEA (0.075 mL, 0.539 mmol).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07407968B2 |
| Quelldatensatz | uspto-grants-2008_08 |
| ORD ID | ord-aae50351a47f408185bf7e833ea1afb0 |
| Quellennotiz | uspto-grants-2008_08 |