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HRID2217942

反应详情

EQUATION

反应方程式

HRID 2217942 的结构方程式

REACTANTS

反应物

2
结构：O.O.[Cl][Sn][Cl]
HCID61436

Stannous chloride dihydrate

Cl2H4O2Sn

结构：O=C(c1ccc(NCc2ccsc2)c([N+](=O)[O-])c1)N(CC(F)(F)F)CC(F)(F)F
HCID58874497

未命名化合物

PRODUCTS

生成物

1
结构：Nc1cc(C(=O)N(CC(F)(F)F)CC(F)(F)F)ccc1NCc1ccsc1
HCID58874480

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

Same procedure used as above using 3-nitro-4-[(3-thienylmethyl)amino]-N,N-bis(2,2,2-trifluoroethyl)benzamide (138 mg, 0.312 mmol) and tin(II) chloride dihydrate (210 mg, 0.936 mmol) in 5 mL of DMF. Yield: 125 mg (97%); MS (ESI) 412.08 (MH+).