참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Acetic Acid | HCID 176 | — |
| 반응물 | N-methyl-N-phenyl-hydrazine | HCID 36299 | — |
| 반응물 | 4-Quinolinecarboxaldehyde | HCID 78072 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Quinoline-4-carbaldehyde methyl(phenyl)hydrazone | HCID 364169 | — |
반응 단계
One equivalent of methylphenylhydrazine (4.1 g; 0.033 mol, compound 2 was diluted in 25 ml of ethanol and 0.5 ml of glacial acetic acid in a three-necked flask on which was mounted a condenser. The reaction medium was then stirred at 0° C. 1 equivalent of 4-formylquinoline (5.28 g; 0.033 mol, compound 14) was added by spatula. After adding the aldehyde, the reaction medium was heated at 70° C. (oil bath temperature) for 4 hours.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07410506B2 |
|---|
| 출처 데이터셋 | uspto-grants-2008_08 |
|---|
| ORD ID | ord-0d071e769ecd4e128c39b2f5485a2956 |
|---|
| 출처 메모 | uspto-grants-2008_08 |
|---|
