HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylboronic Acid → HCID 11774251, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | (2,6-Dimethoxyphenyl)boronic acid | HCID 2734343 | — |
| Reactant | HCID 69287689 | HCID 69287689 | — |
| Product | HCID 11774251 | HCID 11774251 | 71% |
Reaction Steps
Prepared from 3-(7-bromo-1-methyl-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-5-yl)-benzonitrile Intermediate 14 using the same method described for Example 1 and instead of using benzene boronic acid, we used 2,6-dimethoxyphenyl boronic acid. The title compound (148 mg) was obtained as a yellow solid, (yield=71%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07410963B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-985f37a379764a6987597defcda90960 |
| Source note | uspto-grants-2008_08 |