HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorophenylboronic acid → HCID 11371854, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorophenylboronic acid | HCID 74299 | — |
| Reactant | 3-Formylphenylboronic acid | HCID 2734356 | — |
| Reactant | HCID 69289305 | HCID 69289305 | — |
| Product | HCID 11371854 | HCID 11371854 | 35% |
Reaction Steps
Prepared from 5-chloro-1-methyl-7-phenyl-1,3-dihydro-benzo[e][1,4]diazepin-2-one using the same method described for Example 9 and instead of using 3-formylbenzene boronic acid, we used 4-chlorophenyl boronic acid. The title compound was obtained as a pale yellow solid, (yield=35%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07410963B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-600940a6515a455791c5a14388d1db88 |
| Source note | uspto-grants-2008_08 |