HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-butyl N-(prop-2-yn-1-yl)carbamate → HCID 11156469, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-butyl N-(prop-2-yn-1-yl)carbamate | HCID 11073648 | — |
| Reactant | HCID 11487361 | HCID 11487361 | — |
| Product | HCID 11156469 | HCID 11156469 | 22% |
Reaction Steps
Prepared from 5-(3-bromo-phenyl)-8-methoxy-1-methyl-7-phenyl-1,3-dihydro-benzo[e][1,4]diazepin-2-one Example 62 using the same method described for Example 35 using propargyl Boc-amine instead of hex-1-yne. The title compound (51 mg) was obtained as a beige solid, (yield=22%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07410963B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-e3e0778e34c442fba8bc9c1f54392ec8 |
| Source note | uspto-grants-2008_08 |