HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(Benzyl-methyl-amino)-heptan-3-ol → (4-Cyclohexyl-3-hydroxy-butyl)-methyl-carbamic acid tert-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(Benzyl-methyl-amino)-heptan-3-ol | HCID 17981933 | — |
| Reactant | (4-Cyclohexyl-3-oxo-butyl)-methyl-carbamic acid tert-butyl ester | HCID 59769551 | — |
| Product | (4-Cyclohexyl-3-hydroxy-butyl)-methyl-carbamic acid tert-butyl ester | HCID 59769577 | — |
Reaction Steps
Using a method similar to that for 1-(Benzyl-methyl-amino)-heptan-3-ol, (4-cyclohexyl-3-oxo-butyl)-methyl-carbamic acid tert-butyl ester affords the title compound: 1H NMR (CDCl3) δ 3.90-3.80 (m, 1H), 3.62-3.52 (m, 1H), 2.88-2.96 (m, 1H), 2.83 (3H), 1.80-1.60 (m, 6H), 1.56-1.32 (m, 3H), 1.47 (s, 9H), 1.31-1.08 (m, 4H), 0.98-0.77 (m, 2H),
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07410982B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-3f014be0b0a34d108d2c4008ec459f51 |
| Source note | uspto-grants-2008_08 |