HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(4-Hydroxymethylphenyl)acrylic acid ethyl ester → Ethyl 3-(4-(hydroxymethyl)phenyl)propanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(4-Hydroxymethylphenyl)acrylic acid ethyl ester | HCID 68457582 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl 3-(4-(hydroxymethyl)phenyl)propanoate | HCID 14839455 | — |
Reaction Steps
3-(4-Hydroxymethylphenyl)acrylic acid ethyl ester (P4, 3 g, 14.5 mmol) and palladium on charcoal (0.3 g) in ethanol (30 mL) was stirred for 4 hours under atmospheric pressure of hydrogen. The reaction mixture was filtered through celite (Diatomaceous Earth) and concentrated to afford the title compound as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07410984B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-88962a19cc68445dac2f54de163f87b2 |
| Source note | uspto-grants-2008_08 |