HuagongsheHuagongshe Chemistry Print Report · For research reference only
Malononitrile → HCID 69145744, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Malononitrile | HCID 8010 | — |
| Reactant | 3-Hydroxy-4-nitrobenzaldehyde | HCID 69712 | — |
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Reactant | HCID 22258775 | HCID 22258775 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 69145744 | HCID 69145744 | — |
Reaction Steps
A mixture of 2-[(4-methoxybenzyl)oxy]acetophenone, 3-hydroxy-4-nitrobenzaldehyde, malononitrile, ammonium acetate and toluene was stirred under reflux for 3 hrs. The usual work-up and column chromatography gave 2-amino-4-(3-hydroxy-4-nitrophenyl)-6-{2-[(4-methoxybenzyl)oxy]-phenyl}nicotinonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07410986B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-b7c7cdf459e8476cbf4b6d707c7a7cbd |
| Source note | uspto-grants-2008_08 |