Bromine → HCID 178419505, compound

HRID 2218357Notes

Reaction equation

HRID 2218357 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]2[N:10]=[C:9]([C:11]3[CH:16]=[CH:15][C:14]([CH3:17])=[CH:13][CH:12]=3)[NH:8][C:5]2=[N:6][CH:7]=1.[Br:18]Br>C(O)(=O)C>[Br:1][C:2]1[CH:3]=[C:4]2[N:10]=[C:9]([C:11]3[CH:16]=[CH:15][C:14]([CH2:17][Br:18])=[CH:13][CH:12]=3)[NH:8][C:5]2=[N:6][CH:7]=1

Participants

4

Reactant 2

HCID 24408BromineHCID 178423927HCID 178423927, compound

Product 1

HCID 178419505HCID 178419505, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

The title compound was prepared by refluxing 6-bromo-2-(4-methylphenyl)-3H-imidazo[4,5-b]pyridine with a large excess of bromine in acetic acid overnight. APCI-MS m/z: 366/368/370 [MH+].

Sources & evidence

ORD record
ord-b80d298986374d47ae38825311f457a7
Source dataset
uspto-grants-2008_08
Patent number
US07410966B2

Reaction notes

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