3-Cyanobenzene-1-sulfonyl chloride → HCID 69209617, compound

Participants

Reaction Conditions

Reaction Steps

4-(6-Bromo-7-methyl-1H-imidazo[4,5-b]pyridin-2-yl)aniline (Example 260) (0.020 g, 0.07 mmol) was dissolved in pyridine and 3-cyanobenzenesulfonyl chloride (0.013 g, 0.07 mmol) was added. The mixture was heated to 60° C. for 3 h. Thereafter the solvent was removed in vacuo and the residue was submitted to HPLC-C18 purification. Yield: 0.006 g (15%) of the title compound as the trifluoroacetate.

Provenance & Evidence