Dimethylethylamine → HCID 85988700, compound

HRID 2218553Notes

Reaction equation

HRID 2218553 reaction equation
[CH3:1][N:2]([CH3:5])[CH2:3][CH3:4].[Br:6][CH2:7][CH2:8][O:9][CH2:10][CH2:11][O:12][CH3:13]>C(#N)C>[Br-:6].[CH3:1][N+:2]([CH3:5])([CH2:3][CH3:4])[CH2:7][CH2:8][O:9][CH2:10][CH2:11][O:12][CH3:13]

Participants

4

Reactant 2

HCID 11723DimethylethylamineHCID 1235321-Bromo-3,6-dioxaheptane

Product 1

HCID 85988700HCID 85988700, compoundYield 100%

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Conditions

Temperature
80 °C

Procedure

A mixture of 5.12 g (0.070 mol) of dimethylethylamine, 14.2 g (0.070 mol) of 1-bromo-2-(methoxyethoxy)ethane and 10.2 g of acetonitrile was stirred at 80° C. for 24 hours for reaction thereof. After completion of the reaction, the resulted reaction mixture was concentrated, and the residue was dried under reduced pressure to obtain 18.4 g (0.070 mol) of N,N-dimethyl-N-ethyl-N-methoxyethoxyethylammonium bromide.

Workup

  1. customAfter completion of the reaction
  2. customthe resulted reaction mixture
  3. concentrationwas concentrated
  4. customthe residue was dried under reduced pressure

Sources & evidence

ORD record
ord-a402af0360214a28a389e15092b8febc
Source dataset
uspto-grants-2008_08
Patent number
US07411092B2

Reaction notes

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