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HRID221862

反应详情

EQUATION

反应方程式

HRID 221862 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc(NN)cc1
HCID77023

(4-Methoxyphenyl)hydrazine

C7H10N2O

结构：CC(C)(C)c1cc(N)n(-c2ccc(C(=O)O)cc2)n1
HCID974688

4-[5-Amino-3-(1,1-dimethylethyl)-1H-pyrazol-1-yl]benzoic acid

C14H17N3O2

PRODUCTS

生成物

1
结构：COc1ccc(-n2nc(C(C)(C)C)cc2N)cc1
HCID11139395

3-tert-Butyl-1-(4-methoxyphenyl)-1H-pyrazol-5-amine

C14H19N3O

PROCEDURE

实验过程

The title compound was prepared in the same manner as described for 4-(5-amino-3-tert-butyl-pyrazol-1-yl)benzoic acid, replacing 4-hydrazinobenzoic acid with 4-methoxyphenylhydrazine. 1H-NMR (DMSO-d6) δ 7.40 (d, J=5.1 Hz, 2H), 6.98 (d, J=4.8 Hz, 2H), 5.32 (s, 1H), 5.05 (s, 2H), 3.77 (s, 3H), 1.20 (s, 9H); MS LC-MS [M+H]+=246, RT=1.76 min.