HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Propanesulfonyl chloride → HCID 59770521, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Propanesulfonyl chloride | HCID 82408 | — |
| Reactant | HCID 59769900 | HCID 59769900 | — |
| Product | HCID 59770521 | HCID 59770521 | — |
Reaction Steps
Following procedures essentially as described in Example 90, 4-(10,11-dihydro-dibenzo[a,d]cyclohepten-5-ylidenemethyl)-phenylamine (100 mg, 0.336 mmol) and 2-propanesulfonyl chloride (144 mg, 1.01 mmol) affords the title compound. MS (ES) 426 (M+Na), 402 (M−H); HPLC shows 93% purity.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07411072B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-7d03d08fda134ddc8f4330af54fc2e55 |
| Source note | uspto-grants-2008_08 |