2-Methylphenyl boronic acid → HCID 59769953, compound

Participants

Reaction Steps

Combine 5-bromomethylene-10,11-dihydro-5H-dibenzo[a,d]cycloheptene (0.5 g, 1.75 mmol) and o-tolylboronic acid (0.238 g, 1.75 mmol) using procedures essentially as described in Example 219, below. Pass through a plug of silica gel equilibrated with hexanes. Concentrate the filtrate to give the title product: MS (m/e) 296 (M+); Analysis for C23H20: Calcd: C, 93.19 H, 6.80. Found: C, 93.42 H, 6.79.

Provenance & Evidence