HuagongsheHuagongshe Chemistry Print Report · For research reference only
10,11-dihydro-5H-dibenzo(a,d)cycloheptene → HCID 59770364, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 10,11-dihydro-5H-dibenzo(a,d)cycloheptene | HCID 70029 | — |
| Reactant | 4-Fluoro-3-methoxybenzaldehyde | HCID 2737358 | — |
| Product | HCID 59770364 | HCID 59770364 | 49% |
Reaction Steps
Following procedures essentially as described in Example 28 and using 4-fluoro-3-methoxybenzaldehyde (1.59 g, 10.3 mmol), dibenzosuberane (1.94 g, 10 mmol, provides 1.66 g of title compound in 49% yield as a light tan oil that slowly crystallized. HPLC shows 93% purity.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07411072B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-adf68084fb1943fbbf973940ff1b30a2 |
| Source note | uspto-grants-2008_08 |