HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 68937093, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 68937232 | HCID 68937232 | — |
| Product | HCID 68937093 | HCID 68937093 | 69% |
Reaction Steps
Demethylate the corresponding methoxy mixture of Example 161 using BBr3 to give the title compound in 69% yield. MS (ES) 392 (M+1), 390 (M−1). HPLC shows 48% of the faster eluting isomer and 45% of the slower isomer.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07411072B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-98c72efc7f7c4829a042276606b7f136 |
| Source note | uspto-grants-2008_08 |