HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-hydroxyphenyl)boronic Acid → 3-(2-Chloro-10,11-dihydro-dibenzo[a,d]cyclohepten-5-ylidenemethyl)-phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-hydroxyphenyl)boronic Acid | HCID 2734359 | — |
| Reactant | 5-bromomethylene-2-chloro-10,11-dihydro-5H-dibenzo[a,d]cycloheptene | HCID 68886819 | — |
| Product | 3-(2-Chloro-10,11-dihydro-dibenzo[a,d]cyclohepten-5-ylidenemethyl)-phenol | HCID 68935023 | — |
Reaction Steps
Following procedures essentially as described in Example 219, below, and using (3-hydroxyphenyl)boronic acid (108 mg, 0.78 mmol) and 5-bromomethylene-2-chloro-10,11-dihydro-5H-dibenzo[a,d]cycloheptene (209 mg, 0.65 mmol) provides the title compound. Mass Spec (EI+) 332.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07411072B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-e68f922dd8004d77801b2951bb62a311 |
| Source note | uspto-grants-2008_08 |