HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxyphenylboronic acid → 4-(2-Chloro-10,11-dihydro-dibenzo[a,d]cyclohepten-5-ylidenemethyl)-phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxyphenylboronic acid | HCID 2734360 | — |
| Reactant | 5-bromomethylene-2-chloro-10,11-dihydro-5H-dibenzo[a,d]cycloheptene | HCID 68886819 | — |
| Product | 4-(2-Chloro-10,11-dihydro-dibenzo[a,d]cyclohepten-5-ylidenemethyl)-phenol | HCID 68937460 | — |
Reaction Steps
Following procedures essentially as described in Example 219, below, and using (4-hydroxyphenyl)boronic acid (55 mg, 0.40 mmol) and 5-bromomethylene-2-chloro-10,11-dihydro-5H-dibenzo[a,d]cycloheptene (103 mg, 0.32 mmol) provides the title compound. Mass Spec (EI+) 332.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07411072B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-435518cb9f164b0298a563acb265b744 |
| Source note | uspto-grants-2008_08 |