3-Methylsulfonylaminophenylboronic acid → HCID 68935771, compound

HRID 2218750Notes

Reaction equation

HRID 2218750 reaction equation
[CH3:1][C:2]1[S:11][C:10]2[C:9](=[CH2:12])[C:8]3[CH:13]=[CH:14][CH:15]=[CH:16][C:7]=3[CH2:6][CH2:5][C:4]=2[N:3]=1.[CH3:17][S:18]([NH:21][C:22]1[CH:23]=[C:24](B(O)O)[CH:25]=[CH:26][CH:27]=1)(=[O:20])=[O:19]>>[CH3:1][C:2]1[S:11][C:10]2[C:9](=[CH:12][C:26]3[CH:27]=[C:22]([NH:21][S:18]([CH3:17])(=[O:19])=[O:20])[CH:23]=[CH:24][CH:25]=3)[C:8]3[CH:13]=[CH:14][CH:15]=[CH:16][C:7]=3[CH2:6][CH2:5][C:4]=2[N:3]=1

Participants

3

Reactant 2

HCID 27735353-Methylsulfonylaminophenylboronic acidHCID 59769884HCID 59769884, compound

Product 1

HCID 68935771HCID 68935771, compound

Procedure

Following procedures essentially as described in Preparation 24 followed by procedures essentially as described in Example 219, and using 2-methyl-4-methylene-9,10-dihydro-4H-3-thia-1-aza-benzo[f]azulene and 3-methanesulfonylaminophenylboronic acid, the title compounds are made.

Workup

  1. customas described in Preparation 24

Sources & evidence

ORD record
ord-4f66a8b6e2794b278b22b0b5b62db4b2
Source dataset
uspto-grants-2008_08
Patent number
US07411072B2

Reaction notes

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