Aluminium lithium hydride → HCID 59770130, compound

Participants

Reaction Steps

Treat (10,11-dihydro-dibenzo[a,d]cyclohepten-5-ylidene)-(3-methansulfonylamino-phenyl)-acetic acid ethyl ester (1 equivalent) with lithium aluminum hydride (2 equivalents) in a suitable dry solvent and stir at room temperature for four hours. Quench by the dropwise addition of water and partition between dichloromethane and water. Dry the organic layer over anhydrous sodium sulfate and evaporate. Purify the crude residue by silica gel chromatography to obtain a 33% yield on the title compound.

Provenance & Evidence