HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4,4-Dimethylcyclohex-1-enyl)-2-nitrobenzene → 2-(4,4-Dimethylcyclohexyl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4,4-Dimethylcyclohex-1-enyl)-2-nitrobenzene | HCID 23142003 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2-(4,4-Dimethylcyclohexyl)aniline | HCID 15340111 | — |
Reaction Steps
A mixture of 1-(4,4-dimethylcyclohex-1-enyl)-2-nitrobenzene (16.3 g, 70.5 mmol) prepared in Example (3a), 10% palladium on carbon (1 g, wet) and ethyl acetate (100 mL) was stirred for 14 hours and 30 minutes under a hydrogen atmosphere at atmospheric pressure and room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07410971B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-5d1cfb4654e74229a066d35290c70b32 |
| Source note | uspto-grants-2008_08 |