Ethanol → HCID 58794811, compound

HRID 2218925Notes

Reaction equation

HRID 2218925 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([NH:10][CH:11]([CH2:15][CH2:16][CH2:17][CH2:18][NH:19][C:20]2[CH:25]=[CH:24][C:23]([N+:26]([O-:28])=[O:27])=[CH:22][CH:21]=2)[C:12]([OH:14])=[O:13])=[CH:6][CH:5]=1)([O-:3])=[O:2].S(=O)(=O)(O)O.[CH2:34](O)[CH3:35]>>[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([NH:10][CH:11]([CH2:15][CH2:16][CH2:17][CH2:18][NH:19][C:20]2[CH:21]=[CH:22][C:23]([N+:26]([O-:28])=[O:27])=[CH:24][CH:25]=2)[C:12]([O:14][CH2:34][CH3:35])=[O:13])=[CH:6][CH:5]=1)([O-:3])=[O:2]

Participants

4

Reactant 3

HCID 702EthanolHCID 1118Sulfuric AcidHCID 59770609HCID 59770609, compound

Product 1

HCID 58794811HCID 58794811, compound

Procedure

5 g of 2,6-bis[(4-nitrophenyl)amino]hexanoic acid dissolved in 50 ml of ethanol and 1.5 ml of sulphuric acid are introduced into a 100 ml three-necked flask equipped with a condenser and a thermometer, and the mixture is then refluxed overnight.

Workup

  1. customequipped with a condenser
  2. temperaturea thermometer, and the mixture is then refluxed overnight

Sources & evidence

ORD record
ord-a679d8c52ac04dac954f696fdaae0b00
Source dataset
uspto-grants-2008_08
Patent number
US07413580B2

Reaction notes

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