HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11097971, compound → HCID 10152164, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11097971 | HCID 11097971 | — |
| Reactant | HCID 69215565 | HCID 69215565 | — |
| Product | HCID 10152164 | HCID 10152164 | 69% |
Reaction Steps
The same procedure as step 3 of example 1 was accomplished, except for using epoxide compound (450 mg, 1.6 mmol) obtained in step 1 of example 2 and N-(4-fluorophenyl)-N-(2-methyl-2H-tetrazol-5-ylmethyl)amine (332 mg, 1.6 mmol). The crude product was purified by silica gel column chromatography (developing solvent-n-hexane:ethyl acetate=1:1), to give desired compound (528 mg, yield: 69%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07414068B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-f8d7ee560b674a72bd4e043da4de1361 |
| Source note | uspto-grants-2008_08 |