HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11097971, compound → HCID 10288916, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11097971 | HCID 11097971 | — |
| Reactant | HCID 69213675 | HCID 69213675 | — |
| Product | HCID 10288916 | HCID 10288916 | 48% |
Reaction Steps
The same procedure as step 3 of example 1 was accomplished, except for using epoxide compound (200 mg, 0.71 mmol) obtained in step 1 of example 2 and N-benzyl-N-(2-methyl-2H-tetrazol-5-ylmethyl)amine (145 mg, 0.71 mmol). The crude product was purified by silica gel column chromatography (developing solvent-n-hexane:ethyl acetate=1:2), to give desired compound (165 mg, yield: 48%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07414068B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-86dc022ebf1d4078a99de19cd2769ba7 |
| Source note | uspto-grants-2008_08 |