HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-4-fluorophenylboronic Acid (contains varying amounts of Anhydride) → HCID 23725268, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-4-fluorophenylboronic Acid (contains varying amounts of Anhydride) | HCID 2734660 | — |
| Reactant | HCID 178434980 | HCID 178434980 | — |
| Product | HCID 23725268 | HCID 23725268 | 5% |
Reaction Steps
As described for Example 3, 4-(1H-imidazol-4-yl)-5-methyl-3-phenyl-isoxazole (112.6 mg, 0.5 mmol) was converted, using 3-chloro-4-fluorophenylboronic acid instead of 4-fluorophenylboronic acid, to the title compound (8 mg, 5%) which was obtained as a white solid. MS (ESI): m/e=353.9 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07414061B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-29395579dee34daaae894c9be5e16755 |
| Source note | uspto-grants-2008_08 |