HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dichlorobenzeneboronic acid → HCID 23725269, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dichlorobenzeneboronic acid | HCID 2734330 | — |
| Reactant | HCID 178434980 | HCID 178434980 | — |
| Product | HCID 23725269 | HCID 23725269 | 10% |
Reaction Steps
As described for Example 3, 4-(1H-imidazol-4-yl)-5-methyl-3-phenyl-isoxazole (112.6 mg, 0.5 mmol) was converted, using 3,4-dichlorophenylboronic acid instead of 4-fluorophenylboronic acid, to the title compound (18 mg, 10%) which was obtained as a white solid. MS (ESI): m/e=369.9 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07414061B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-952679bf26fe4ff69914b29909072162 |
| Source note | uspto-grants-2008_08 |