HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Fluoronitrobenzene → HCID 23725860, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Fluoronitrobenzene | HCID 9590 | — |
| Reactant | HCID 178438221 | HCID 178438221 | — |
| Product | HCID 23725860 | HCID 23725860 | 30% |
Reaction Steps
As described for Example 30 e), 5-ethyl-4-(1H-imidazol-4-yl)-3-phenyl-isoxazole (100 mg, 0.43 mmol) was converted using 1-fluoro-4-nitro-benzene instead of 4-fluoroacetophenone to the title compound (45 mg, 30%) which was obtained as a white solid. MS: m/e=347.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07414061B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-6c37f0544357475182481b857a2f90b7 |
| Source note | uspto-grants-2008_08 |