HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloropyrimidine → HCID 23725963, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloropyrimidine | HCID 74404 | — |
| Reactant | HCID 178434980 | HCID 178434980 | — |
| Product | HCID 23725963 | HCID 23725963 | 68% |
Reaction Steps
As described for Example 12, 4-(1H-imidazol-4-yl)-5-methyl-3-phenyl-isoxazole (100 mg, 0.44 mmol) using 2-chloropyrimidine instead of 4-fluoroacetophenone was converted to the title compound (92 mg, 68%) which was obtained as an off-white solid. MS: m/e=304.0 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07414061B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-460f6220cf874c118d1637c8f763fd45 |
| Source note | uspto-grants-2008_08 |