HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propargylamine → HCID 86613560, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propargylamine | HCID 239041 | — |
| Reactant | HCID 67421132 | HCID 67421132 | — |
| Product | HCID 86613560 | HCID 86613560 | 25% |
Reaction Steps
As described for Example 71, prop-2-ynylamine was converted, using 2-[4-(5-methyl-3-phenyl-isoxazol-4-yl)-imidazol-1-yl]-benzoic acid (100 mg, 0.29 mmol) instead of 4-[4-(5-methyl-3-phenyl-isoxazol-4-yl)-imidazol-1-yl]-benzoic acid, to the title compound (28 mg, 25%) which was obtained as an off-white solid. MS: m/e=383.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07414061B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-97486076caeb42a6a2aa1810421823e3 |
| Source note | uspto-grants-2008_08 |