HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Fluoronitrobenzene → HCID 23725532, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Fluoronitrobenzene | HCID 9590 | — |
| Reactant | HCID 178438222 | HCID 178438222 | — |
| Product | HCID 23725532 | HCID 23725532 | 28% |
Reaction Steps
As described for 1f, 1-fluoro-4-nitro-benzene was converted, using 5-ethyl-3-(4-fluoro-phenyl)-4-(1H-imidazole-4-yl)-isoxazole (100 mg, 0.39 mmol) instead of 4-(1H-imidazol-4-yl)-3-phenyl-isoxazole was converted to the title compound (43 mg, 28%) which was obtained as an off-white solid. MS: m/e=379.1.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07414061B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-294422c58ea54aa98fe10ecf2c51c4e8 |
| Source note | uspto-grants-2008_08 |