HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzonitrile → HCID 69275465, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzonitrile | HCID 14517 | — |
| Reactant | HCID 178494752 | HCID 178494752 | — |
| Product | HCID 69275465 | HCID 69275465 | 42% |
Reaction Steps
As described for Example 1f, 3-phenyl-4-(1H-imidazol-4-yl)-5-methoxymethyl-isoxazole (128 mg, 0.50 mmol) was converted, using 4-fluorobenzonitrile instead of 1-(4-fluorophenyl)-ethanone, to the title compound (75 mg, 42%) which was obtained as an off-white solid. MS: m/e=357.0[M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07414061B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-2fe2a6d90736439da7796d91990caef9 |
| Source note | uspto-grants-2008_08 |