HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromobenzyl alcohol → HCID 23725639, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromobenzyl alcohol | HCID 85141 | — |
| Reactant | HCID 23725534 | HCID 23725534 | — |
| Product | HCID 23725639 | HCID 23725639 | 61% |
Reaction Steps
As described for Example 157, 4-[2-chloromethyl-1-(4-nitro-phenyl)-1H-imidazol-4-yl]-5-methyl-3-phenyl-isoxazole (100 mg, 0.25 mmol), using 3-bromobenzyl alcohol instead of 3-chlorobenzyl alcohol, was converted to the title compound (84 mg, 61%) which was obtained as a light yellow gum. MS: m/e=545.3/547.3 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07414061B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-7fa203a067a3482581544d52b578703a |
| Source note | uspto-grants-2008_08 |